Crystallography Open Database

Information card for entry 7063487

Preview

Coordinates	7063487.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H46 Cl3 N4 O Rh
Calculated formula	C33 H46 Cl3 N4 O Rh
Title of publication	Rhodium complexes bearing 2-(pyridin-2-yl)hydrazino acenaphthene-1-one: synthesis, structure and electrochemical studies
Authors of publication	Bakaev, I. V.; Komlyagina, V. I.; Ulantikov, A. A.; Romashev, N. F.; Gushchin, A. L.
Journal of publication	New Journal of Chemistry
Year of publication	2024
Journal volume	48
Journal issue	43
Pages of publication	18456 - 18464
a	29.0387 ± 0.0018 Å
b	10.4088 ± 0.0006 Å
c	11.1178 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	3360.4 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0711
Residual factor for significantly intense reflections	0.0441
Weighted residual factors for significantly intense reflections	0.0898
Weighted residual factors for all reflections included in the refinement	0.1003
Goodness-of-fit parameter for all reflections included in the refinement	0.999
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296632 (current)	2024-12-06	cif/ Updating files of 7063486, 7063487 Original log message: Adding full bibliography for 7063486--7063487.cif.	7063487.cif
295451	2024-10-12	cif/ Adding structures of 7063486, 7063487 via cif-deposit CGI script.	7063487.cif