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Information card for entry 7102146
Preview
| Coordinates | 7102146.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C86 H124 N4 O2 Pb2 |
|---|---|
| Calculated formula | C86 H124 N4 O2 Pb2 |
| SMILES | [Pb]1(Oc2c(cccc2C(C)(C)C)C(C)(C)C)[N](=C(C)C=C(N1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C |
| Title of publication | A new type of heteroleptic complex of divalent lead and synthesis of the P-plumbyleniophosphasilene, R2Si=P‒Pb(L): (L = β-diketiminate) |
| Authors of publication | Yao, Shenglai; Block, Stefan; Brym, Markus; Driess, Matthias |
| Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
| Year of publication | 2007 |
| Journal issue | 37 |
| Pages of publication | 3844 - 3846 |
| a | 19.6849 ± 0.0006 Å |
| b | 10.9636 ± 0.0004 Å |
| c | 36.7625 ± 0.0012 Å |
| α | 90° |
| β | 91.304 ± 0.001° |
| γ | 90° |
| Cell volume | 7931.9 ± 0.5 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0672 |
| Residual factor for significantly intense reflections | 0.0445 |
| Weighted residual factors for significantly intense reflections | 0.1029 |
| Weighted residual factors for all reflections included in the refinement | 0.1122 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 209731 (current) | 2018-08-15 | cif/7/ Updating bibliography in entries 7102146-7102149, 7113240-7113243. Marking entries 7113240-7113243 as duplicates of entries 7102146-7102149. |
7102146.cif |
| 180123 | 2016-03-26 | cif/7/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/10/21. |
7102146.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7102146.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7102146.cif |
| 966 | 2010-01-30 | cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated. |
7102146.cif |
| 403 | 2008-06-25 | Comitting the Chem-Comm-2007/ CIF files with extracted structural data. |
7102146.cif |
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