Crystallography Open Database

Information card for entry 7111350

Preview

Coordinates	7111350.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H105 N O8 V2
Calculated formula	C68 H105 N O8 V2
Title of publication	Vanadyl complexes bearing bi- and triphenolate chelate ligands: highly active ethylene polymerisation procatalystsElectronic supplementary information (ESI) available: selected spectroscopic and polymerisation data. See http://www.rsc.org/suppdata/cc/b4/b406783e/
Authors of publication	Redshaw, Carl; Warford, Lee; Dale, Sophie H.; Elsegood, Mark R. J.
Journal of publication	Chemical Communications
Year of publication	2004
Journal issue	17
Pages of publication	1954 - 1955
a	10.6383 ± 0.0012 Å
b	12.7094 ± 0.0014 Å
c	14.6822 ± 0.0016 Å
α	73.299 ± 0.002°
β	76.055 ± 0.002°
γ	70.891 ± 0.002°
Cell volume	1772.8 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0938
Residual factor for significantly intense reflections	0.0701
Weighted residual factors for significantly intense reflections	0.2003
Weighted residual factors for all reflections included in the refinement	0.2245
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180227 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/13.	7111350.cif
96445	2014-01-29	cif/ Adding structures of 7111350, 7111351 via cif-deposit CGI script.	7111350.cif