Crystallography Open Database

Information card for entry 7111732

Preview

Coordinates	7111732.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H47 Cl4 Eu N8 O9
Calculated formula	C52 H41 Cl4 Eu N8 O8
Title of publication	Dipyridyl β-diketonate complexes: versatile polydentate metalloligands for metal‒organic frameworks and hydrogen-bonded networks
Authors of publication	Burrows, Andrew D.; Frost, Christopher G.; Mahon, Mary F.; Raithby, Paul R.; Renouf, Catherine L.; Richardson, Christopher; Stevenson, Anna J.
Journal of publication	Chemical Communications
Year of publication	2010
Journal volume	46
Journal issue	28
Pages of publication	5067 - 5069
a	15.107 ± 0.0004 Å
b	27.386 ± 0.0007 Å
c	29.038 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	12013.6 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	70
Hermann-Mauguin space group symbol	F d d d :2
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.0602
Residual factor for significantly intense reflections	0.0502
Weighted residual factors for significantly intense reflections	0.1079
Weighted residual factors for all reflections included in the refinement	0.1123
Goodness-of-fit parameter for all reflections included in the refinement	1.192
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180231 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/17.	7111732.cif
96754	2014-01-29	cif/ Adding structures of 7111729, 7111730, 7111731, 7111732 via cif-deposit CGI script.	7111732.cif