Crystallography Open Database

Information card for entry 7111750

Preview

Coordinates	7111750.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H48 Cl4 Fe4 P4 Sn4
Calculated formula	C52 H49 Cl4 Fe4 P4 Sn4.12
Title of publication	Stoichiometric and catalytic Sn-mediated dehydrocoupling of primary phosphines
Authors of publication	Naseri, Vesal; Less, Robert J.; Mulvey, Robert E.; McPartlin, Mary; Wright, Dominic S.
Journal of publication	Chemical Communications
Year of publication	2010
Journal volume	46
Journal issue	27
Pages of publication	5000 - 5002
a	18.245 ± 0.004 Å
b	15.165 ± 0.003 Å
c	19.997 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	5533 ± 2 Å³
Cell temperature	260 ± 2 K
Ambient diffraction temperature	260 ± 2 K
Number of distinct elements	6
Space group number	63
Hermann-Mauguin space group symbol	C m c m
Hall space group symbol	-C 2c 2
Residual factor for all reflections	0.0568
Residual factor for significantly intense reflections	0.0363
Weighted residual factors for significantly intense reflections	0.0891
Weighted residual factors for all reflections included in the refinement	0.1002
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180231 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/17.	7111750.cif
96763	2014-01-29	cif/ Adding structures of 7111748, 7111749, 7111750 via cif-deposit CGI script.	7111750.cif