Crystallography Open Database

Information card for entry 7112981

Preview

Coordinates	7112981.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H38 N2 P2 Si2 Tl2
Calculated formula	C31 H38 N2 P2 Si2 Tl2
Title of publication	A geminal dithallated bis(iminodiphenylphosphorano)methine carbon bridged dimer bound by Tl-Tl interactions.
Authors of publication	Ma, Guibin; Ferguson, Michael J.; Cavell, Ronald G.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2010
Journal volume	46
Journal issue	29
Pages of publication	5370 - 5372
a	14.0949 ± 0.0012 Å
b	13.1494 ± 0.0011 Å
c	18.9302 ± 0.0016 Å
α	90°
β	91.764 ± 0.001°
γ	90°
Cell volume	3506.9 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0219
Residual factor for significantly intense reflections	0.0195
Weighted residual factors for significantly intense reflections	0.0483
Weighted residual factors for all reflections included in the refinement	0.0493
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180243 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/29.	7112981.cif
112195	2014-04-30	cif/ Adding structures of 7112981 via cif-deposit CGI script.	7112981.cif