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Information card for entry 7114294
Preview
| Coordinates | 7114294.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | [Bert*Ge(C6H10)(mu-C6H10)]2 |
|---|---|
| Formula | C90 H128 Ge2 |
| Calculated formula | C90 H128 Ge2 |
| Title of publication | Formation of [Ar*Ge{CH2C(Me)C(Me)CH2}CH2C(Me)]2 (Ar* = C6H3-2,6-Trip2; Trip = C6H2-2,4,6-i-Pr3) via reaction of Ar*GeGeAr* with 2,3-dimethyl-1,3-butadiene: evidence for the existence of a germanium analogue of an alkyne |
| Authors of publication | Stender, Matthias; Phillips, Andrew D.; Power, Philip P. |
| Journal of publication | Chemical Communications |
| Year of publication | 2002 |
| Journal issue | 12 |
| Pages of publication | 1312 |
| a | 12.8612 ± 0.0008 Å |
| b | 19.4797 ± 0.0012 Å |
| c | 16.8275 ± 0.001 Å |
| α | 90° |
| β | 106.828 ± 0.001° |
| γ | 90° |
| Cell volume | 4035.3 ± 0.4 Å3 |
| Cell temperature | 90 ± 2 K |
| Ambient diffraction temperature | 90 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0991 |
| Residual factor for significantly intense reflections | 0.0671 |
| Weighted residual factors for significantly intense reflections | 0.1581 |
| Weighted residual factors for all reflections included in the refinement | 0.177 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180256 (current) | 2016-03-26 | cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/42. |
7114294.cif |
| 116665 | 2014-06-13 | cif/ Adding structures of 7114294 via cif-deposit CGI script. |
7114294.cif |
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Users of the data should acknowledge the original authors of the
structural data.