Crystallography Open Database

Information card for entry 7118822

Preview

Coordinates	7118822.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Fe(cinammic hydroxamate)3]
Formula	C28.8 H30.2 Fe N3 O7.3
Calculated formula	C28.8 H30.2 Fe N3 O7.3
Title of publication	Phosphinosilylenes as a novel ligand system for heterobimetallic complexes.
Authors of publication	Breit, Nora C.; Eisenhut, Carsten; Inoue, Shigeyoshi
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	32
Pages of publication	5523 - 5526
a	16.0853 ± 0.0015 Å
b	28.696 ± 0.003 Å
c	7.0062 ± 0.0006 Å
α	90°
β	96.758 ± 0.003°
γ	90°
Cell volume	3211.5 ± 0.5 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1101
Residual factor for significantly intense reflections	0.0729
Weighted residual factors for significantly intense reflections	0.1747
Weighted residual factors for all reflections included in the refinement	0.1899
Goodness-of-fit parameter for all reflections included in the refinement	1.105
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
182615 (current)	2016-05-06	cif/ Updating files of 7118819, 7118820, 7118821, 7118822 Original log message: Adding full bibliography for 7118819--7118822.cif.	7118822.cif
177104	2016-03-02	cif/ Adding structures of 7118819, 7118820, 7118821, 7118822 via cif-deposit CGI script.	7118822.cif