Crystallography Open Database

Information card for entry 7122379

Preview

Coordinates	7122379.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	RuSb6-cluster
Formula	C70 H118 K2 N4 O12 Ru2 Sb6
Calculated formula	C70 H118 K2 N4 O12 Ru2 Sb6
Title of publication	The cyclo-Sb<sub>6</sub> ring in the [Sb<sub>6</sub>(RuCp*)<sub>2</sub>]<sup>2-</sup> ion.
Authors of publication	Wang, Yi; Zavalij, Peter; Eichhorn, Bryan
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	84
Pages of publication	11917 - 11920
a	13.0477 ± 0.0011 Å
b	14.1374 ± 0.0012 Å
c	23.62 ± 0.002 Å
α	87.7781 ± 0.0014°
β	84.4934 ± 0.0013°
γ	79.1444 ± 0.0014°
Cell volume	4258.3 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0371
Residual factor for significantly intense reflections	0.0248
Weighted residual factors for significantly intense reflections	0.0552
Weighted residual factors for all reflections included in the refinement	0.0572
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
228478 (current)	2019-11-17	cif/ Updating files of 7122378, 7122379 Original log message: Adding full bibliography for 7122378--7122379.cif.	7122379.cif
211183	2018-09-27	cif/ Adding structures of 7122378, 7122379 via cif-deposit CGI script.	7122379.cif