Crystallography Open Database

Information card for entry 7124907

Preview

Coordinates	7124907.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H59 N O3 Si Zn
Calculated formula	C47 H59 N O3 Si Zn
Title of publication	Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
Authors of publication	Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	69
Pages of publication	10490 - 10492
a	21.1923 ± 0.0012 Å
b	21.1923 ± 0.0012 Å
c	18.9615 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	8515.9 ± 1 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.0908
Residual factor for significantly intense reflections	0.0543
Weighted residual factors for significantly intense reflections	0.1238
Weighted residual factors for all reflections included in the refinement	0.1477
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
234338 (current)	2019-11-23	cif/ Adding structures of 7124906, 7124907, 7124908, 7124909, 7124910, 7124911, 7124912, 7124913, 7124914 via cif-deposit CGI script.	7124907.cif