Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7129675
Preview
| Coordinates | 7129675.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C40 H56 Li2 N2 Si2 |
|---|---|
| Calculated formula | C40 H56 Li2 N2 Si2 |
| Title of publication | Tetracyclic silaheterocycle formed through a pericyclic reaction cascade including a two-fold intramolecular C–C bond activation |
| Authors of publication | Lips, Felicitas; Helmer, Joschua; Pakkanen, Olli J.; Gendy, Chris; Hepp, Alexander; Tuononen, Heikki M. |
| Journal of publication | Chemical Communications |
| Year of publication | 2022 |
| a | 11.5185 ± 0.0004 Å |
| b | 12.592 ± 0.0005 Å |
| c | 12.8943 ± 0.0005 Å |
| α | 90° |
| β | 91.928 ± 0.001° |
| γ | 90° |
| Cell volume | 1869.14 ± 0.12 Å3 |
| Cell temperature | 116 ± 2 K |
| Ambient diffraction temperature | 116 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0509 |
| Residual factor for significantly intense reflections | 0.0433 |
| Weighted residual factors for significantly intense reflections | 0.1221 |
| Weighted residual factors for all reflections included in the refinement | 0.1275 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.011 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 272842 (current) | 2022-02-08 | cif/ Adding structures of 7129675, 7129676, 7129677, 7129678, 7129679 via cif-deposit CGI script. |
7129675.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.