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Information card for entry 7129962
Preview
| Coordinates | 7129962.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C69 H110 N3 Na O6 Si Zn |
|---|---|
| Calculated formula | C69 H110 N3 Na O6 Si Zn |
| Title of publication | Metallation of sensitive fluoroarenes using a potassium TMP-zincate supported by a silyl(bis)amido ligand |
| Authors of publication | Mastropierro, Pasquale; Kennedy, Alan R.; Hevia, Eva |
| Journal of publication | Chemical Communications |
| Year of publication | 2022 |
| a | 10.4753 ± 0.0001 Å |
| b | 35.3408 ± 0.0005 Å |
| c | 37.566 ± 0.0005 Å |
| α | 87.637 ± 0.001° |
| β | 82.661 ± 0.001° |
| γ | 88.947 ± 0.001° |
| Cell volume | 13780.3 ± 0.3 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0738 |
| Residual factor for significantly intense reflections | 0.0615 |
| Weighted residual factors for significantly intense reflections | 0.1656 |
| Weighted residual factors for all reflections included in the refinement | 0.1776 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 274452 (current) | 2022-04-12 | cif/ Adding structures of 7129958, 7129959, 7129960, 7129961, 7129962, 7129963, 7129964, 7129965, 7129966, 7129967, 7129968 via cif-deposit CGI script. |
7129962.cif |
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Users of the data should acknowledge the original authors of the
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