Crystallography Open Database

Information card for entry 7130341

Preview

Coordinates	7130341.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C252 H252 N6 O72 Rh12
Calculated formula	C252 H252 N6 O72 Rh12
Title of publication	Synthesis of the Two Isomers of Heteroleptic Rh12L6L’6 Metal-Organic Polyhedra by Screening of Complementary Linkers
Authors of publication	Broto-Ribas, Anna; Gutiérrez, Susana; Imaz, Inhar; Carné-Sánchez, Arnau; Gándara, Felipe; Juanhuix, Judith; Maspoch, Daniel
Journal of publication	Chemical Communications
Year of publication	2022
a	31.6843 ± 0.0005 Å
b	31.6843 ± 0.0005 Å
c	72.349 ± 0.002 Å
α	90°
β	90°
γ	120°
Cell volume	62900 ± 2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	167
Hermann-Mauguin space group symbol	R -3 c :H
Hall space group symbol	-R 3 2"c
Residual factor for all reflections	0.1354
Residual factor for significantly intense reflections	0.1105
Weighted residual factors for significantly intense reflections	0.3237
Weighted residual factors for all reflections included in the refinement	0.3509
Goodness-of-fit parameter for all reflections included in the refinement	1.245
Diffraction radiation wavelength	0.82656 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
276785 (current)	2022-07-23	cif/ Adding structures of 7130335, 7130336, 7130337, 7130338, 7130339, 7130340, 7130341, 7130342, 7130343, 7130344, 7130345, 7130346 via cif-deposit CGI script.	7130341.cif