Crystallography Open Database

Information card for entry 7131539

Preview

Coordinates	7131539.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C138 H276 Co8 F20 N14 Na8 Si28
Calculated formula	C138 H276 Co8 F20 N14 Na8 Si28
Title of publication	Applying Na/Co(II) bimetallic partnerships to promote multiple Co-H exchanges in polyfluoroarenes.
Authors of publication	Logallo, Alessandra; Hevia, Eva
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2023
Journal volume	59
Journal issue	36
Pages of publication	5383 - 5386
a	21.6543 ± 0.0002 Å
b	17.95986 ± 0.00012 Å
c	27.5932 ± 0.0003 Å
α	90°
β	97.4528 ± 0.001°
γ	90°
Cell volume	10640.6 ± 0.17 Å³
Cell temperature	173.01 ± 0.1 K
Ambient diffraction temperature	173.01 ± 0.1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0873
Residual factor for significantly intense reflections	0.0539
Weighted residual factors for significantly intense reflections	0.1261
Weighted residual factors for all reflections included in the refinement	0.1484
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283114 (current)	2023-05-05	cif/ Updating files of 7131535, 7131536, 7131537, 7131538, 7131539 Original log message: Adding full bibliography for 7131535--7131539.cif.	7131539.cif
282592	2023-04-12	cif/ Adding structures of 7131535, 7131536, 7131537, 7131538, 7131539 via cif-deposit CGI script.	7131539.cif