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Information card for entry 7132535
Preview
| Coordinates | 7132535.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C76 H70 Cl8 Ga2 N10 O P4 |
|---|---|
| Calculated formula | C76 H70 Cl8 Ga2 N10 O P4 |
| Title of publication | Addition and NN bond cleavage of diazo-compounds by phosphino-phosphenium cations. |
| Authors of publication | Kim, Hyehwang; Lough, Alan; Qu, Zheng-Wang; Grimme, Stefan; Stephan, Douglas W. |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 8 |
| Pages of publication | 1031 - 1034 |
| a | 9.9147 ± 0.0007 Å |
| b | 18.9028 ± 0.0013 Å |
| c | 23.475 ± 0.0017 Å |
| α | 68.039 ± 0.003° |
| β | 85.656 ± 0.003° |
| γ | 76.81 ± 0.003° |
| Cell volume | 3972.5 ± 0.5 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0642 |
| Residual factor for significantly intense reflections | 0.0532 |
| Weighted residual factors for significantly intense reflections | 0.1339 |
| Weighted residual factors for all reflections included in the refinement | 0.142 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 289330 (current) | 2024-02-04 | cif/ Updating files of 7132534, 7132535, 7132536, 7132537, 7132538 Original log message: Adding full bibliography for 7132534--7132538.cif. |
7132535.cif |
| 288482 | 2023-12-22 | cif/ Adding structures of 7132534, 7132535, 7132536, 7132537, 7132538 via cif-deposit CGI script. |
7132535.cif |
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Users of the data should acknowledge the original authors of the
structural data.