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Information card for entry 7132585
Preview
| Coordinates | 7132585.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C116 H128 N8 O24 S8 |
|---|---|
| Calculated formula | C116 H128 N8 O24 S8 |
| Title of publication | Iridium-catalysed hydroamination of internal homoallylic amines. |
| Authors of publication | Ho, An T.; Vanable, Evan P.; Miguel, Chelsea San; Hull, Kami L. |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 12 |
| Pages of publication | 1615 - 1618 |
| a | 15.6273 ± 0.0006 Å |
| b | 11.1454 ± 0.0004 Å |
| c | 21.3411 ± 0.0008 Å |
| α | 90° |
| β | 104.896 ± 0.002° |
| γ | 90° |
| Cell volume | 3592.1 ± 0.2 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100.15 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0713 |
| Residual factor for significantly intense reflections | 0.0528 |
| Weighted residual factors for significantly intense reflections | 0.1675 |
| Weighted residual factors for all reflections included in the refinement | 0.1824 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.0911 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 290107 (current) | 2024-03-04 | cif/ Updating files of 7132585, 7132586 Original log message: Adding full bibliography for 7132585--7132586.cif. |
7132585.cif |
| 288680 | 2024-01-05 | cif/ Adding structures of 7132585, 7132586 via cif-deposit CGI script. |
7132585.cif |
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Users of the data should acknowledge the original authors of the
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