Crystallography Open Database

Information card for entry 7132726

Preview

Coordinates	7132726.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H48 N10 P2 U
Calculated formula	C20 H48 N10 P2 U
Title of publication	Temperature induced single-crystal to single-crystal transformation of uranium azide complexes.
Authors of publication	Li, Kai; Rajeshkumar, Thayalan; Zhao, Yue; Wang, Tianwei; Maron, Laurent; Zhu, Congqing
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	21
Pages of publication	2966 - 2969
a	10.1931 ± 0.0014 Å
b	10.6719 ± 0.001 Å
c	14.9477 ± 0.0017 Å
α	90°
β	102.736 ± 0.004°
γ	90°
Cell volume	1586 ± 0.3 Å³
Cell temperature	353 K
Ambient diffraction temperature	353 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1059
Residual factor for significantly intense reflections	0.0455
Weighted residual factors for significantly intense reflections	0.1032
Weighted residual factors for all reflections included in the refinement	0.127
Goodness-of-fit parameter for all reflections included in the refinement	0.906
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
290831 (current)	2024-04-05	cif/ Updating files of 7132717, 7132718, 7132719, 7132720, 7132721, 7132722, 7132723, 7132724, 7132725, 7132726, 7132727, 7132728, 7132729 Original log message: Adding full bibliography for 7132717--7132729.cif.	7132726.cif
289848	2024-02-17	cif/ Adding structures of 7132717, 7132718, 7132719, 7132720, 7132721, 7132722, 7132723, 7132724, 7132725, 7132726, 7132727, 7132728, 7132729 via cif-deposit CGI script.	7132726.cif