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Information card for entry 7132842
Preview
| Coordinates | 7132842.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H24 O2 |
|---|---|
| Calculated formula | C18 H24 O2 |
| Title of publication | Divergent synthesis of multi-substituted phenanthrenes <i>via</i> an internal redox reaction/ring expansion sequence. |
| Authors of publication | Koyama, Ryosei; Anada, Masahiro; Sueki, Shunsuke; Makino, Kosho; Kojima, Tatsuhiro; Kawasaki-Takasuka, Tomoko; Mori, Keiji |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 28 |
| Pages of publication | 3822 - 3825 |
| a | 9.864 ± 0.0001 Å |
| b | 9.8656 ± 0.0001 Å |
| c | 16.5931 ± 0.0002 Å |
| α | 105.165 ± 0.001° |
| β | 97.065 ± 0.001° |
| γ | 105.295 ± 0.001° |
| Cell volume | 1471 ± 0.03 Å3 |
| Cell temperature | 101 ± 1 K |
| Ambient diffraction temperature | 101 ± 1 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0416 |
| Residual factor for significantly intense reflections | 0.0378 |
| Weighted residual factors for significantly intense reflections | 0.0993 |
| Weighted residual factors for all reflections included in the refinement | 0.1024 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 290804 (current) | 2024-04-05 | cif/ Updating files of 7132841, 7132842 Original log message: Adding full bibliography for 7132841--7132842.cif. |
7132842.cif |
| 290460 | 2024-03-13 | cif/ Adding structures of 7132841, 7132842 via cif-deposit CGI script. |
7132842.cif |
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Users of the data should acknowledge the original authors of the
structural data.