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Information card for entry 7133135
Preview
| Coordinates | 7133135.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H27 F3 O7 S |
|---|---|
| Calculated formula | C24 H27 F3 O7 S |
| Title of publication | Macrocyclization of carbon dioxide with 3-triflyloxybenzynes and tetrahydrofuran: straightforward access to 14-membered macrolactones. |
| Authors of publication | Liu, Hongjian; Jiang, Huanfeng; Qi, Chaorong |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 52 |
| Pages of publication | 6639 - 6642 |
| a | 13.4729 ± 0.0008 Å |
| b | 13.6729 ± 0.0008 Å |
| c | 14.874 ± 0.0008 Å |
| α | 65.885 ± 0.002° |
| β | 84.653 ± 0.002° |
| γ | 77.547 ± 0.002° |
| Cell volume | 2442 ± 0.2 Å3 |
| Cell temperature | 171 K |
| Ambient diffraction temperature | 171 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1601 |
| Residual factor for significantly intense reflections | 0.0694 |
| Weighted residual factors for significantly intense reflections | 0.1373 |
| Weighted residual factors for all reflections included in the refinement | 0.1819 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 292798 (current) | 2024-07-05 | cif/ Updating files of 7133133, 7133134, 7133135 Original log message: Adding full bibliography for 7133133--7133135.cif. |
7133135.cif |
| 292178 | 2024-06-05 | cif/ Adding structures of 7133133, 7133134, 7133135 via cif-deposit CGI script. |
7133135.cif |
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Users of the data should acknowledge the original authors of the
structural data.