Crystallography Open Database

Information card for entry 7133284

Preview

Coordinates	7133284.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H21 N O6 S
Calculated formula	C21 H21 N O6 S
Title of publication	Catalytic enantioselective [3+2] and [4+2]-annulation of cyclic <i>N</i>-sulfonyl ketimines with γ- or δ-hydroxy-α,β-unsaturated ketones.
Authors of publication	Yang, Ji Seon; Kim, Sung-Gon
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	61
Pages of publication	7954 - 7957
a	8.4145 ± 0.0003 Å
b	8.4145 ± 0.0003 Å
c	56.119 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	3973.4 ± 0.3 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.1172
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.0918
Weighted residual factors for all reflections included in the refinement	0.1172
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
293717 (current)	2024-08-05	cif/ Updating files of 7133283, 7133284 Original log message: Adding full bibliography for 7133283--7133284.cif.	7133284.cif
292734	2024-07-05	cif/ Adding structures of 7133283, 7133284 via cif-deposit CGI script.	7133284.cif