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Information card for entry 7134365
Preview
| Coordinates | 7134365.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H34 N2 O2 |
|---|---|
| Calculated formula | C30 H34 N2 O2 |
| Title of publication | Reductive alkylation of azoarenes to N-alkylated hydrazines enabled by hexafluoroisopropanol |
| Authors of publication | Das, Animesh; Senapati, Siddhartha Kumar |
| Journal of publication | Chemical Communications |
| Year of publication | 2025 |
| a | 11.5525 ± 0.0008 Å |
| b | 7.9187 ± 0.0006 Å |
| c | 28.056 ± 0.002 Å |
| α | 90° |
| β | 96.854 ± 0.002° |
| γ | 90° |
| Cell volume | 2548.2 ± 0.3 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1246 |
| Residual factor for significantly intense reflections | 0.0994 |
| Weighted residual factors for significantly intense reflections | 0.2239 |
| Weighted residual factors for all reflections included in the refinement | 0.2439 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.142 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 298654 (current) | 2025-03-30 | cif/ Adding structures of 7134365 via cif-deposit CGI script. |
7134365.cif |
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Users of the data should acknowledge the original authors of the
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