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Information card for entry 7134641
Preview
Coordinates | 7134641.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H39 Al N2 |
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Calculated formula | C28 H39 Al N2 |
Title of publication | Alkylaluminium-catalyzed regioselective hydrophosphinylation of α,β-unsaturated ketones into γ-ketophosphine oxides |
Authors of publication | Chen, Yiwen; Pang, Ziyuan; Li, Gege; Yang, Xiaobo; Yan, Wenliang; Li, Qifeng; Dong, Xuan; Ma, Xiaoli; Yang, Zhi |
Journal of publication | Chemical Communications |
Year of publication | 2025 |
Journal volume | 61 |
Journal issue | 53 |
Pages of publication | 9666 - 9669 |
a | 16.5787 ± 0.0004 Å |
b | 20.7155 ± 0.0004 Å |
c | 29.815 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 10239.5 ± 0.4 Å3 |
Cell temperature | 99.9 ± 0.2 K |
Ambient diffraction temperature | 99.9 ± 0.2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0692 |
Residual factor for significantly intense reflections | 0.0461 |
Weighted residual factors for significantly intense reflections | 0.1108 |
Weighted residual factors for all reflections included in the refinement | 0.1184 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
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300428 (current) | 2025-07-06 | cif/ Updating files of 7134639, 7134640, 7134641, 7134642 Original log message: Adding full bibliography for 7134639--7134642.cif. |
7134641.cif |
299879 | 2025-05-31 | cif/ Adding structures of 7134639, 7134640, 7134641, 7134642 via cif-deposit CGI script. |
7134641.cif |
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Users of the data should acknowledge the original authors of the
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