Crystallography Open Database

Information card for entry 7156239

Preview

Coordinates	7156239.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C99 H100 N2 O3
Calculated formula	C99 H100 N2 O3
Title of publication	Modular synthesis of heptaarylindole.
Authors of publication	Suzuki, Shin; Asako, Takashi; Itami, Kenichiro; Yamaguchi, Junichiro
Journal of publication	Organic & biomolecular chemistry
Year of publication	2018
Journal volume	16
Journal issue	20
Pages of publication	3771 - 3776
a	13.339 ± 0.005 Å
b	18.203 ± 0.006 Å
c	18.304 ± 0.007 Å
α	106.445 ± 0.004°
β	110.829 ± 0.006°
γ	95.262 ± 0.006°
Cell volume	3891 ± 2 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2317
Residual factor for significantly intense reflections	0.0936
Weighted residual factors for significantly intense reflections	0.2036
Weighted residual factors for all reflections included in the refinement	0.286
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
230767 (current)	2019-11-17	cif/ Updating files of 7156239, 7156240, 7156241, 7156242, 7156243 Original log message: Adding full bibliography for 7156239--7156243.cif.	7156239.cif
207650	2018-05-03	cif/ Adding structures of 7156239, 7156240, 7156241, 7156242, 7156243 via cif-deposit CGI script.	7156239.cif