Crystallography Open Database

Information card for entry 7156541

Preview

Coordinates	7156541.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H19 N O3
Calculated formula	C24 H19 N O3
Title of publication	Oxidative cross-dehydrogenative [2 + 3] annulation of α-amino ketones with α-keto esters: concise synthesis of clausenamide analogues.
Authors of publication	Bhajammanavar, Vinod; Mallik, Sumitava; Baidya, Mahiuddin
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	17
Journal issue	7
Pages of publication	1740 - 1743
a	5.8336 ± 0.0006 Å
b	11.4947 ± 0.0015 Å
c	14.982 ± 0.002 Å
α	77.575 ± 0.005°
β	81.412 ± 0.005°
γ	77.375 ± 0.004°
Cell volume	951.8 ± 0.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.085
Residual factor for significantly intense reflections	0.0512
Weighted residual factors for significantly intense reflections	0.1273
Weighted residual factors for all reflections included in the refinement	0.151
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
225205 (current)	2019-11-08	cif/ Updating files of 7156541 Original log message: Adding full bibliography for 7156541.cif.	7156541.cif
211721	2018-10-31	cif/ Adding structures of 7156541 via cif-deposit CGI script.	7156541.cif