Crystallography Open Database

Information card for entry 7157245

Preview

Coordinates	7157245.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H33 Cl N2 O5
Calculated formula	C38 H33 Cl N2 O5
Title of publication	Diastereoselective construction of carbazole-based spirooxindoles via the Levy three-component reaction.
Authors of publication	Zhan, Shao-Cong; Sun, Jing; Liu, Ru-Zhang; Yan, Chao-Guo
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	18
Journal issue	1
Pages of publication	163 - 168
a	13.4926 ± 0.0007 Å
b	9.4573 ± 0.0005 Å
c	25.3206 ± 0.0014 Å
α	90°
β	91.8378 ± 0.0017°
γ	90°
Cell volume	3229.3 ± 0.3 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0975
Residual factor for significantly intense reflections	0.0519
Weighted residual factors for significantly intense reflections	0.1063
Weighted residual factors for all reflections included in the refinement	0.1245
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
247801 (current)	2020-02-04	cif/ Updating files of 7157234, 7157235, 7157236, 7157237, 7157238, 7157239, 7157240, 7157241, 7157242, 7157243, 7157244, 7157245, 7157246, 7157247 Original log message: Adding full bibliography for 7157234--7157247.cif.	7157245.cif
244876	2019-12-03	cif/ Adding structures of 7157234, 7157235, 7157236, 7157237, 7157238, 7157239, 7157240, 7157241, 7157242, 7157243, 7157244, 7157245, 7157246, 7157247 via cif-deposit CGI script.	7157245.cif