Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7157270
Preview
Coordinates | 7157270.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34 H52 O2 |
---|---|
Calculated formula | C34 H52 O2 |
Title of publication | Palladium catalyzed synthesis of benzannulated steroid spiroketals. |
Authors of publication | Mayorquín-Torres, Martha C; González-Orozco, Juan Carlos; Flores-Álamo, Marcos; Camacho-Arroyo, Ignacio; Iglesias-Arteaga, Martín A |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2020 |
Journal volume | 18 |
Journal issue | 4 |
Pages of publication | 725 - 737 |
a | 7.4753 ± 0.0005 Å |
b | 8.3777 ± 0.0007 Å |
c | 23.7615 ± 0.0017 Å |
α | 90° |
β | 97.224 ± 0.006° |
γ | 90° |
Cell volume | 1476.27 ± 0.19 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 3 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0736 |
Residual factor for significantly intense reflections | 0.0527 |
Weighted residual factors for significantly intense reflections | 0.1152 |
Weighted residual factors for all reflections included in the refinement | 0.1417 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
247813 (current) | 2020-02-04 | cif/ Updating files of 7157265, 7157266, 7157267, 7157268, 7157269, 7157270 Original log message: Adding full bibliography for 7157265--7157270.cif. |
7157270.cif |
245423 | 2019-12-20 | cif/ Adding structures of 7157265, 7157266, 7157267, 7157268, 7157269, 7157270 via cif-deposit CGI script. |
7157270.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.