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Information card for entry 7157422
Preview
Coordinates | 7157422.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H33 O3 P |
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Calculated formula | C26 H33 O3 P |
Title of publication | Stereoselective preparation of P,axial-stereogenic allenyl bisphosphine oxides via chirality-transfer. |
Authors of publication | Qiu, Mao-Ran; Zheng, Hong-Xing; Ye, Jing-Jing; Yan, Bing-Xia; Zhao, Chang-Qiu; Li, Qiang |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2020 |
Journal volume | 18 |
Journal issue | 16 |
Pages of publication | 3017 - 3021 |
a | 8.8154 ± 0.0007 Å |
b | 11.3911 ± 0.0009 Å |
c | 24.121 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2422.2 ± 0.3 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0773 |
Residual factor for significantly intense reflections | 0.0443 |
Weighted residual factors for significantly intense reflections | 0.0963 |
Weighted residual factors for all reflections included in the refinement | 0.1113 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
251719 (current) | 2020-05-05 | cif/ Updating files of 7157420, 7157421, 7157422 Original log message: Adding full bibliography for 7157420--7157422.cif. |
7157422.cif |
249728 | 2020-03-26 | cif/ Adding structures of 7157420, 7157421, 7157422 via cif-deposit CGI script. |
7157422.cif |
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Users of the data should acknowledge the original authors of the
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