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Information card for entry 7157426
Preview
| Coordinates | 7157426.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C25 H29 N O4 |
|---|---|
| Calculated formula | C25 H29 N O4 |
| Title of publication | Chiral diene-promoted room temperature conjugate arylation: highly enantioselective synthesis of substituted chiral phenylalanine derivatives and α,α-di(arylmethyl)acetates. |
| Authors of publication | Chen, Jian-Ping; Xu, Ming-Hua |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2020 |
| Journal volume | 18 |
| Journal issue | 24 |
| Pages of publication | 4569 - 4574 |
| a | 9.0309 ± 0.0004 Å |
| b | 13.028 ± 0.0005 Å |
| c | 19.9637 ± 0.0008 Å |
| α | 99.064 ± 0.002° |
| β | 98.729 ± 0.002° |
| γ | 91.614 ± 0.002° |
| Cell volume | 2289.36 ± 0.16 Å3 |
| Cell temperature | 173 K |
| Ambient diffraction temperature | 173 K |
| Number of distinct elements | 4 |
| Space group number | 1 |
| Hermann-Mauguin space group symbol | P 1 |
| Hall space group symbol | P 1 |
| Residual factor for all reflections | 0.072 |
| Residual factor for significantly intense reflections | 0.0702 |
| Weighted residual factors for significantly intense reflections | 0.2066 |
| Weighted residual factors for all reflections included in the refinement | 0.211 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 253972 (current) | 2020-07-06 | cif/ Updating files of 7157426, 7157427 Original log message: Adding full bibliography for 7157426--7157427.cif. |
7157426.cif |
| 249779 | 2020-03-27 | cif/ Adding structures of 7157426, 7157427 via cif-deposit CGI script. |
7157426.cif |
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Users of the data should acknowledge the original authors of the
structural data.