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Information card for entry 7157491
Preview
| Coordinates | 7157491.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C45 H74 N2 O20 S2 |
|---|---|
| Calculated formula | C45 H74 N2 O20 S2 |
| Title of publication | Synthesis of glycosyl sulfoximines by a highly chemo- and stereoselective NH- and O-transfer to thioglycosides. |
| Authors of publication | Tota, Arianna; Carlucci, Claudia; Pisano, Luisa; Cutolo, Giuliano; Clarkson, Guy J.; Romanazzi, Giuseppe; Degennaro, Leonardo; Bull, James A.; Rollin, Patrick; Luisi, Renzo |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2020 |
| Journal volume | 18 |
| Journal issue | 20 |
| Pages of publication | 3893 - 3897 |
| a | 9.74142 ± 0.00005 Å |
| b | 9.74142 ± 0.00005 Å |
| c | 55.7588 ± 0.0004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 5291.25 ± 0.05 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 96 |
| Hermann-Mauguin space group symbol | P 43 21 2 |
| Hall space group symbol | P 4nw 2abw |
| Residual factor for all reflections | 0.0469 |
| Residual factor for significantly intense reflections | 0.0464 |
| Weighted residual factors for significantly intense reflections | 0.1189 |
| Weighted residual factors for all reflections included in the refinement | 0.1193 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 252920 (current) | 2020-06-05 | cif/ Updating files of 7157491 Original log message: Adding full bibliography for 7157491.cif. |
7157491.cif |
| 251531 | 2020-05-05 | cif/ Adding structures of 7157491 via cif-deposit CGI script. |
7157491.cif |
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Users of the data should acknowledge the original authors of the
structural data.