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Information card for entry 7157854
Preview
| Coordinates | 7157854.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H20 O3 S |
|---|---|
| Calculated formula | C24 H20 O3 S |
| Title of publication | Synthesis of C3-sulfone substituted naphthols <i>via</i> rhodium(III)-catalyzed annulation of sulfoxonium ylides with alkynylsulfones. |
| Authors of publication | Xie, Wucheng; Jian, Xinyi; Zhang, Liyang; Jin, Kexin; Shi, Junjun; Zhu, Feng |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2021 |
| Journal volume | 19 |
| Journal issue | 7 |
| Pages of publication | 1498 - 1502 |
| a | 8.1695 ± 0.0006 Å |
| b | 11.1838 ± 0.0009 Å |
| c | 12.1869 ± 0.001 Å |
| α | 116.288 ± 0.008° |
| β | 102.125 ± 0.007° |
| γ | 97.876 ± 0.006° |
| Cell volume | 941.83 ± 0.16 Å3 |
| Cell temperature | 99.98 ± 0.1 K |
| Ambient diffraction temperature | 99.98 ± 0.1 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0546 |
| Residual factor for significantly intense reflections | 0.0441 |
| Weighted residual factors for significantly intense reflections | 0.1087 |
| Weighted residual factors for all reflections included in the refinement | 0.1163 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 262726 (current) | 2021-03-05 | cif/ Updating files of 7157853, 7157854 Original log message: Adding full bibliography for 7157853--7157854.cif. |
7157854.cif |
| 261256 | 2021-01-27 | cif/ Adding structures of 7157853, 7157854 via cif-deposit CGI script. |
7157854.cif |
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Users of the data should acknowledge the original authors of the
structural data.