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Information card for entry 7157999
Preview
Coordinates | 7157999.cif |
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Original paper (by DOI) | HTML |
Formula | C25 H35 N O7 |
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Calculated formula | C25 H35 N O7 |
Title of publication | Lewis acid mediated cyclization: synthesis of 2 spirocyclohexylindolines. |
Authors of publication | Kong, Xiang-Kai; Xiong, Zhi-Min; Zhi, Xiang; Meng, Xue-Ling; Zhao, Jing-Feng; Chen, Wen; Zhang, Hongbin |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2021 |
Journal volume | 19 |
Journal issue | 18 |
Pages of publication | 4043 - 4047 |
a | 10.8932 ± 0.0002 Å |
b | 17.0966 ± 0.0003 Å |
c | 39.2989 ± 0.0007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7318.9 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0353 |
Residual factor for significantly intense reflections | 0.0328 |
Weighted residual factors for significantly intense reflections | 0.0821 |
Weighted residual factors for all reflections included in the refinement | 0.084 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
266173 (current) | 2021-06-05 | cif/ Updating files of 7157995, 7157996, 7157997, 7157998, 7157999, 7158000, 7158001 Original log message: Adding full bibliography for 7157995--7158001.cif. |
7157999.cif |
263480 | 2021-03-31 | cif/ Adding structures of 7157995, 7157996, 7157997, 7157998, 7157999, 7158000, 7158001 via cif-deposit CGI script. |
7157999.cif |
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Users of the data should acknowledge the original authors of the
structural data.