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Information card for entry 7158474
Preview
| Coordinates | 7158474.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H29 N O Si |
|---|---|
| Calculated formula | C18 H29 N O Si |
| SMILES | [Si](CC1(c2ccccc2N(C1)C(=O)C)C)(CC)(CC)CC |
| Title of publication | Copper-Promoted Difunctionalization of Unactivated Alkenes with Silanes |
| Authors of publication | Xue, Yingying; Guo, Zhuangzhuang; Chen, Xiaoyu; Li, Jingya; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2022 |
| a | 22.3463 ± 0.0008 Å |
| b | 7.5222 ± 0.0003 Å |
| c | 22.4194 ± 0.0011 Å |
| α | 90° |
| β | 102.133 ± 0.004° |
| γ | 90° |
| Cell volume | 3684.4 ± 0.3 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0606 |
| Residual factor for significantly intense reflections | 0.047 |
| Weighted residual factors for significantly intense reflections | 0.1276 |
| Weighted residual factors for all reflections included in the refinement | 0.1415 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 271807 (current) | 2022-01-05 | cif/ Adding structures of 7158474 via cif-deposit CGI script. |
7158474.cif |
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