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Information card for entry 7158505
Preview
| Coordinates | 7158505.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H30 N2 O2 S |
|---|---|
| Calculated formula | C27 H30 N2 O2 S |
| Title of publication | Enantioselective synthesis of 2-indolyl methanamine derivatives through disulfonimide-catalyzed Friedel-Crafts C2-alkylation of 3-substituted indoles with imines. |
| Authors of publication | Sun, Peng; Jia, Zi-Hao; Tang, Li; Zheng, Hao; Li, Zhang-Rui; Chen, Ling-Yan; Li, Ya |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2022 |
| Journal volume | 20 |
| Journal issue | 9 |
| Pages of publication | 1916 - 1925 |
| a | 9.4321 ± 0.0003 Å |
| b | 14.6668 ± 0.0005 Å |
| c | 17.7584 ± 0.0006 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2456.67 ± 0.14 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0393 |
| Residual factor for significantly intense reflections | 0.0338 |
| Weighted residual factors for significantly intense reflections | 0.0831 |
| Weighted residual factors for all reflections included in the refinement | 0.0871 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273434 (current) | 2022-03-05 | cif/ Updating files of 7158505 Original log message: Adding full bibliography for 7158505.cif. |
7158505.cif |
| 272440 | 2022-02-03 | cif/ Adding structures of 7158505 via cif-deposit CGI script. |
7158505.cif |
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Users of the data should acknowledge the original authors of the
structural data.