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Information card for entry 7159295
Preview
| Coordinates | 7159295.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C19 H26 F N O4 Si |
|---|---|
| Calculated formula | C19 H26 F N O4 Si |
| SMILES | O=C1N2CC[C@@H]([C@@]2(c2cccc(c12)F)O[Si](C)(C)C(C)(C)C)C(=O)OC.O=C1N2CC[C@H]([C@]2(c2cccc(c12)F)O[Si](C)(C)C(C)(C)C)C(=O)OC |
| Title of publication | Tetramate derivatives by chemoselective Dieckmann ring closure of <i>allo</i>-phenylserines, and their antibacterial activity. |
| Authors of publication | Saney, Liban; Christensen, Kirsten E.; Genov, Miroslav; Pretsch, Alexander; Pretsch, Dagmar; Moloney, Mark G. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2023 |
| Journal volume | 21 |
| Journal issue | 19 |
| Pages of publication | 4061 - 4071 |
| a | 7.607 ± 0.0003 Å |
| b | 7.9569 ± 0.0003 Å |
| c | 18.7476 ± 0.0006 Å |
| α | 92.034 ± 0.003° |
| β | 92.705 ± 0.003° |
| γ | 115.382 ± 0.004° |
| Cell volume | 1022.12 ± 0.07 Å3 |
| Cell temperature | 150 K |
| Ambient diffraction temperature | 150 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0435 |
| Residual factor for significantly intense reflections | 0.0399 |
| Weighted residual factors for all reflections | 0.115 |
| Weighted residual factors for significantly intense reflections | 0.1109 |
| Weighted residual factors for all reflections included in the refinement | 0.115 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.0023 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284309 (current) | 2023-06-05 | cif/ Updating files of 7159291, 7159292, 7159293, 7159294, 7159295, 7159296, 7159297, 7159298, 7159299, 7159300, 7159301 Original log message: Adding full bibliography for 7159291--7159301.cif. |
7159295.cif |
| 282644 | 2023-04-15 | cif/ Adding structures of 7159291, 7159292, 7159293, 7159294, 7159295, 7159296, 7159297, 7159298, 7159299, 7159300, 7159301 via cif-deposit CGI script. |
7159295.cif |
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Users of the data should acknowledge the original authors of the
structural data.