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Information card for entry 7159309
Preview
| Coordinates | 7159309.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H25 N O7 |
|---|---|
| Calculated formula | C23 H25 N O7 |
| Title of publication | Nitronate-aryne cycloaddition as a concise route to stereochemically complex fused benzisoxazolines and amino alcohols. |
| Authors of publication | Lukoyanov, Alexander A.; Tabolin, Andrey A.; Nelyubina, Yulia V.; Aksenova, Svetlana A.; Sukhorukov, Alexey Yu |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2023 |
| Journal volume | 21 |
| Journal issue | 18 |
| Pages of publication | 3871 - 3880 |
| a | 8.269 ± 0.0002 Å |
| b | 11.3776 ± 0.0003 Å |
| c | 12.621 ± 0.0003 Å |
| α | 65.347 ± 0.001° |
| β | 81.305 ± 0.002° |
| γ | 82.114 ± 0.002° |
| Cell volume | 1063.13 ± 0.05 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0477 |
| Residual factor for significantly intense reflections | 0.0384 |
| Weighted residual factors for significantly intense reflections | 0.0852 |
| Weighted residual factors for all reflections included in the refinement | 0.0981 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.094 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284325 (current) | 2023-06-05 | cif/ Updating files of 7159308, 7159309, 7159310, 7159311, 7159312, 7159313, 7159314, 7159315 Original log message: Adding full bibliography for 7159308--7159315.cif. |
7159309.cif |
| 282786 | 2023-04-21 | cif/ Adding structures of 7159308, 7159309, 7159310, 7159311, 7159312, 7159313, 7159314, 7159315 via cif-deposit CGI script. |
7159309.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
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Users of the data should acknowledge the original authors of the
structural data.