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Information card for entry 7159322
Preview
| Coordinates | 7159322.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H28 O5 Si |
|---|---|
| Calculated formula | C18 H28 O5 Si |
| Title of publication | An expedient copper-catalysed asymmetric synthesis of γ-lactones and γ-lactams. Application to the synthesis of lucidulactone A. |
| Authors of publication | Ojo, O. Stephen; Hughes, David L.; Richards, Christopher J. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2023 |
| Journal volume | 21 |
| Journal issue | 19 |
| Pages of publication | 4144 - 4149 |
| a | 7.1914 ± 0.0004 Å |
| b | 10.5484 ± 0.0005 Å |
| c | 24.6032 ± 0.0013 Å |
| α | 90° |
| β | 91.051 ± 0.004° |
| γ | 90° |
| Cell volume | 1866.03 ± 0.17 Å3 |
| Cell temperature | 100 ± 0.11 K |
| Ambient diffraction temperature | 100.01 ± 0.1 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0667 |
| Residual factor for significantly intense reflections | 0.0481 |
| Weighted residual factors for significantly intense reflections | 0.0988 |
| Weighted residual factors for all reflections included in the refinement | 0.1049 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284311 (current) | 2023-06-05 | cif/ Updating files of 7159321, 7159322 Original log message: Adding full bibliography for 7159321--7159322.cif. |
7159322.cif |
| 282816 | 2023-04-25 | cif/ Adding structures of 7159321, 7159322 via cif-deposit CGI script. |
7159322.cif |
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Users of the data should acknowledge the original authors of the
structural data.