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Information card for entry 7159564
Preview
| Coordinates | 7159564.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H21 Cl O2 |
|---|---|
| Calculated formula | C26 H21 Cl O2 |
| Title of publication | Selective electrophilic cyclization of <i>ortho</i>-carbonylarylacetylenols for the synthesis of cyclopenta[<i>a</i>]naphthalenol and 2-phenylnaphthalen-1-ol analogs. |
| Authors of publication | Jantrapirom, Jantra; Yongpanich, Phornphan; Tummatorn, Jumreang; Chainok, Kittipong; Jiajaroen, Suwadee; Thongsornkleeb, Charnsak; Ruchirawat, Somsak |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2023 |
| Journal volume | 21 |
| Journal issue | 42 |
| Pages of publication | 8500 - 8515 |
| a | 8.9346 ± 0.0005 Å |
| b | 10.7463 ± 0.0006 Å |
| c | 11.7878 ± 0.0006 Å |
| α | 67.915 ± 0.002° |
| β | 80.436 ± 0.002° |
| γ | 65.89 ± 0.001° |
| Cell volume | 957.15 ± 0.09 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0434 |
| Residual factor for significantly intense reflections | 0.0429 |
| Weighted residual factors for significantly intense reflections | 0.12 |
| Weighted residual factors for all reflections included in the refinement | 0.1204 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.089 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Diffraction radiation X-ray symbol | K-L~3~ |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 287410 (current) | 2023-11-06 | cif/ Updating files of 7159563, 7159564, 7159565 Original log message: Adding full bibliography for 7159563--7159565.cif. |
7159564.cif |
| 286256 | 2023-09-07 | cif/ Adding structures of 7159563, 7159564, 7159565 via cif-deposit CGI script. |
7159564.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
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.
Users of the data should acknowledge the original authors of the
structural data.