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Information card for entry 7159767
Preview
| Coordinates | 7159767.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C38 H28 O4 S4 |
|---|---|
| Calculated formula | C38 H28 O4 S4 |
| Title of publication | l-Proline-catalysed synthesis of 2-aryl-2H,5H-thiopyrano[2,3-b] thiochromen-5-ones from 4-hydroxydithiocoumarins and cinnamaldehyde derivatives |
| Authors of publication | Ali, Ahmad; Faraz, Simra; Khan, Abu Taleb |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2024 |
| Journal volume | 22 |
| Journal issue | 7 |
| Pages of publication | 1426 - 1433 |
| a | 7.6579 ± 0.001 Å |
| b | 13.884 ± 0.0019 Å |
| c | 14.998 ± 0.002 Å |
| α | 87.216 ± 0.003° |
| β | 89.61 ± 0.004° |
| γ | 83.982 ± 0.003° |
| Cell volume | 1584 ± 0.4 Å3 |
| Cell temperature | 297 ± 2 K |
| Ambient diffraction temperature | 297 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0513 |
| Residual factor for significantly intense reflections | 0.0426 |
| Weighted residual factors for significantly intense reflections | 0.1016 |
| Weighted residual factors for all reflections included in the refinement | 0.1087 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 290268 (current) | 2024-03-04 | cif/ Updating files of 7159767 Original log message: Adding full bibliography for 7159767.cif. |
7159767.cif |
| 289047 | 2024-01-12 | cif/ Adding structures of 7159767 via cif-deposit CGI script. |
7159767.cif |
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Users of the data should acknowledge the original authors of the
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