Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7159846
Preview
| Coordinates | 7159846.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H25 N O5 |
|---|---|
| Calculated formula | C33 H25 N O5 |
| Title of publication | Vinylogous and stereoselective domino synthesis of pyrano[2,3-<i>c</i>]pyrroles from alkylidene meldrum's acids. |
| Authors of publication | Savchuk, Mariia; Vo-Thanh, Giang; Oudeyer, Sylvain; Beucher, Hélène; Brière, Jean-François |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2024 |
| Journal volume | 22 |
| Journal issue | 15 |
| Pages of publication | 2948 - 2952 |
| a | 10.1201 ± 0.0002 Å |
| b | 11.3054 ± 0.0003 Å |
| c | 13.5515 ± 0.0003 Å |
| α | 70.37 ± 0.001° |
| β | 72.458 ± 0.001° |
| γ | 67.802 ± 0.001° |
| Cell volume | 1324.77 ± 0.05 Å3 |
| Cell temperature | 300 ± 2 K |
| Ambient diffraction temperature | 300 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0655 |
| Residual factor for significantly intense reflections | 0.052 |
| Weighted residual factors for significantly intense reflections | 0.1389 |
| Weighted residual factors for all reflections included in the refinement | 0.1512 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.059 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 291695 (current) | 2024-05-05 | cif/ Updating files of 7159846 Original log message: Adding full bibliography for 7159846.cif. |
7159846.cif |
| 290439 | 2024-03-12 | cif/ Adding structures of 7159846 via cif-deposit CGI script. |
7159846.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.