Crystallography Open Database

Information card for entry 7216575

Preview

Coordinates	7216575.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H88 As2 N4 O36 V10
Calculated formula	C64 H88 As2 N4 O36 V10
Title of publication	The first example of a novel one-dimensional cyclic tetrameric metavanadate: [PPh4]2V4O11
Authors of publication	Sharma, Sanjeev; Ramanan, Arunachalam; Zavalij, Peter Y.; Whittingham, M. Stanley
Journal of publication	CrystEngComm
Year of publication	2002
Journal volume	4
Journal issue	100
Pages of publication	601
a	10.4005 ± 0.0004 Å
b	11.8621 ± 0.0005 Å
c	17.3981 ± 0.0007 Å
α	97.621 ± 0.001°
β	90.256 ± 0.001°
γ	111.417 ± 0.001°
Cell volume	1977.31 ± 0.14 Å³
Cell temperature	297 ± 2 K
Ambient diffraction temperature	297 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0412
Residual factor for significantly intense reflections	0.0338
Weighted residual factors for significantly intense reflections	0.0862
Weighted residual factors for all reflections included in the refinement	0.0901
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180496 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/65.	7216575.cif
116858	2014-06-14	cif/ Adding structures of 7216575, 7216576 via cif-deposit CGI script.	7216575.cif