Crystallography Open Database

Information card for entry 7216753

Preview

Coordinates	7216753.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H31 Cl4 N2 Pd Sb
Calculated formula	C24 H31 Cl4 N2 Pd Sb
SMILES	c12c(cccc1)C[N](C)(C)[Sb]2(c1ccccc1)(Cl)[Pd](Cl)(Cl)Cl.c1(ccccc1)C[NH+](C)C
Title of publication	Palladium(ii) complexes with chiral organoantimony(iii) ligands. Solution behaviour and solid state structures
Authors of publication	Copolovici, Dana; Isaia, Francesco; Breunig, Hans J.; Raţ, Ciprian I.; Silvestru, Cristian
Journal of publication	RSC Advances
Year of publication	2014
Journal volume	4
Journal issue	51
Pages of publication	26569
a	8.7797 ± 0.0009 Å
b	10.3772 ± 0.0011 Å
c	15.8911 ± 0.0017 Å
α	98.954 ± 0.002°
β	102.05 ± 0.002°
γ	96.987 ± 0.002°
Cell volume	1380.7 ± 0.3 Å³
Cell temperature	297 ± 2 K
Ambient diffraction temperature	297 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0797
Residual factor for significantly intense reflections	0.0648
Weighted residual factors for significantly intense reflections	0.1129
Weighted residual factors for all reflections included in the refinement	0.1175
Goodness-of-fit parameter for all reflections included in the refinement	1.249
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180498 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/67.	7216753.cif
118000	2014-06-23	cif/ Adding structures of 7216751, 7216752, 7216753, 7216754 via cif-deposit CGI script.	7216753.cif