Crystallography Open Database

Information card for entry 7217277

Preview

Coordinates	7217277.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	catena-poly[diaquabis-μ-{N, N-bis(3-pyridyl)butanediamido}copper (II) perchlorate dihydrate]
Formula	C32 H44 Cl2 Cu N8 O16
Calculated formula	C32 H44 Cl2 Cu N8 O16
Title of publication	Is Metal Metathesis a Framework-Templating Strategy to Synthesize Coordination Polymers? Transmetallation Studies involving Flexible ligands
Authors of publication	Suman, Kumari; Baig, Fayaz; Kant, Rajani; Gupta, Vivek; Mandal, Sanjay; Sarkar, Madhushree
Journal of publication	RSC Advances
Year of publication	2014
a	11.3423 ± 0.0003 Å
b	19.2826 ± 0.0007 Å
c	9.5549 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	2089.74 ± 0.11 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	18
Hermann-Mauguin space group symbol	P 21 21 2
Hall space group symbol	P 2 2ab
Residual factor for all reflections	0.0853
Residual factor for significantly intense reflections	0.0679
Weighted residual factors for significantly intense reflections	0.1726
Weighted residual factors for all reflections included in the refinement	0.1867
Goodness-of-fit parameter for all reflections included in the refinement	0.972
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7217277.cif
120991	2014-07-31	cif/ Adding structures of 7217276, 7217277 via cif-deposit CGI script.	7217277.cif