Crystallography Open Database

Information card for entry 7217790

Preview

Coordinates	7217790.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H39 Cl Ge N9 S3 Sm
Calculated formula	C12 H39 Cl Ge N9 S3 Sm
Title of publication	Solvothermal syntheses of lanthanide thiogermanates displaying three new structural moieties
Authors of publication	Zhao, Rongqing; Zhou, Jian; Liu, Xing; Zhang, Li; Tang, Qiuling; Tan, XiaoFeng
Journal of publication	RSC Advances
Year of publication	2014
a	11.532 ± 0.003 Å
b	14.423 ± 0.004 Å
c	14.573 ± 0.004 Å
α	90°
β	97.105 ± 0.005°
γ	90°
Cell volume	2405.3 ± 1.1 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0274
Residual factor for significantly intense reflections	0.0245
Weighted residual factors for significantly intense reflections	0.0647
Weighted residual factors for all reflections included in the refinement	0.0667
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180508 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/77.	7217790.cif
122270	2014-08-20	cif/ Adding structures of 7217789, 7217790, 7217791, 7217792, 7217793 via cif-deposit CGI script.	7217790.cif