Crystallography Open Database

Information card for entry 7219347

7219346 << 7219347 >> 7219348

Preview

Coordinates	7219347.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C77 H70 Cl Ir2 N8 O19 Pb
Calculated formula	C77 H70 Cl Ir2 N8 O19 Pb
Title of publication	Four new lead(ii)‒iridium(iii) heterobimetallic coordination frameworks: synthesis, structures, luminescence and oxygen-sensing properties
Authors of publication	Chen, Yi-Ting; Lin, Chun-Yen; Lee, Gene-Hsiang; Ho, Mei-Lin
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	10
Pages of publication	2129
a	13.1493 ± 0.0004 Å
b	16.19 ± 0.0005 Å
c	19.3364 ± 0.0006 Å
α	66.7678 ± 0.001°
β	70.8605 ± 0.0009°
γ	87.8194 ± 0.0009°
Cell volume	3553.78 ± 0.19 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0971
Residual factor for significantly intense reflections	0.0672
Weighted residual factors for significantly intense reflections	0.1801
Weighted residual factors for all reflections included in the refinement	0.2108
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180524 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/93.	7219347.cif
133178	2015-03-06	cif/ Updating files of 7219347, 7219348, 7219349, 7219350 Original log message: Adding full bibliography for 7219347--7219350.cif.	7219347.cif
130026	2015-01-22	cif/ Adding structures of 7219347, 7219348, 7219349, 7219350 via cif-deposit CGI script.	7219347.cif