Crystallography Open Database

Information card for entry 7219539

7219538 << 7219539 >> 7219540

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Coordinates	7219539.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H49 N2 O Tl
Calculated formula	C32 H49 N2 O Tl
Title of publication	The 13 group metal complexes of sterically-hindered substituted iminophenol. Synthesis and structure.
Authors of publication	Egorova, Elena; Druzhkov, Nikolai; Shavyrin, Andrey; Cherkasov, Anton; Abakumov, Gleb Arsent'evich; Fedorov, Alexey
Journal of publication	RSC Adv.
Year of publication	2015
a	9.485 ± 0.0006 Å
b	9.6118 ± 0.0006 Å
c	17.0918 ± 0.0011 Å
α	90°
β	98.3 ± 0.001°
γ	90°
Cell volume	1541.9 ± 0.17 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0187
Residual factor for significantly intense reflections	0.0167
Weighted residual factors for significantly intense reflections	0.0393
Weighted residual factors for all reflections included in the refinement	0.0399
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180526 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/95.	7219539.cif
131709	2015-02-11	cif/ Adding structures of 7219537, 7219538, 7219539 via cif-deposit CGI script.	7219539.cif