Crystallography Open Database

Information card for entry 7224374

Preview

Coordinates	7224374.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H96 O12 Si12
Calculated formula	C60 H96 O12 Si12
Title of publication	Synthesis and structure of new polyhedral Ni, Na- and Cu, Na-metallasiloxanes with tolyl substituent at the silicon atom
Authors of publication	Anisimov, Anton A.; Kononevich, Yuriy N.; Zhemchugov, Pavel V.; Milenin, Sergey A.; Korlyukov, Alexander A.; Tsareva, Ul'yana S.; Peregudov, Alexander S.; Dorovatovskii, Pavel V.; Molodtsova, Yuliya A.; Takazova, Rina U.; Shchegolikhina, Olga I.; Muzafarov, Aziz M.
Journal of publication	RSC Adv.
Year of publication	2016
Journal volume	6
Journal issue	26
Pages of publication	22052
a	12.919 ± 0.0006 Å
b	13.675 ± 0.0006 Å
c	23.8149 ± 0.0011 Å
α	76.271 ± 0.0011°
β	77.6651 ± 0.0011°
γ	74.0613 ± 0.001°
Cell volume	3880 ± 0.3 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1656
Residual factor for significantly intense reflections	0.0771
Weighted residual factors for significantly intense reflections	0.146
Weighted residual factors for all reflections included in the refinement	0.1851
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176857 (current)	2016-02-24	cif/ Adding structures of 7224373, 7224374, 7224375, 7224376 via cif-deposit CGI script.	7224374.cif