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Information card for entry 7225709
Preview
| Coordinates | 7225709.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C20 H40 O3 Si |
|---|---|
| Calculated formula | C20 H40 O3 Si |
| Title of publication | [3,3]-Sigmatropic rearrangement mediated synthesis of chiral building blocks for the preparation of Gemini and its analogs |
| Authors of publication | Pazos, Gonzalo; Pérez, Manuel; Gándara, Zoila; Gómez, Generosa; Fall, Yagamare |
| Journal of publication | RSC Adv. |
| Year of publication | 2016 |
| Journal volume | 6 |
| Journal issue | 66 |
| Pages of publication | 61073 |
| a | 7.199 ± 0.003 Å |
| b | 11.837 ± 0.005 Å |
| c | 25.842 ± 0.01 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2202.1 ± 1.6 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.096 |
| Residual factor for significantly intense reflections | 0.0435 |
| Weighted residual factors for significantly intense reflections | 0.0932 |
| Weighted residual factors for all reflections included in the refinement | 0.1149 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.997 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 183929 (current) | 2016-06-25 | cif/ Adding structures of 7225709 via cif-deposit CGI script. |
7225709.cif |
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Users of the data should acknowledge the original authors of the
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