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Information card for entry 7227482
Preview
| Coordinates | 7227482.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H72 Cu2 N16 O82 P2 W24 |
|---|---|
| Calculated formula | C44 H64 Cu2 N16 O82 P2 W24 |
| Title of publication | Using a flexible bis(pyrazol) ligand to construct four new Keggin-based compounds: syntheses, structures and properties |
| Authors of publication | Tian, Aixiang; Ni, Huaiping; Ji, Xuebin; Tian, Yan; Liu, Guocheng; Ying, Jun |
| Journal of publication | RSC Adv. |
| Year of publication | 2017 |
| Journal volume | 7 |
| Journal issue | 10 |
| Pages of publication | 5774 |
| a | 12.444 ± 0.002 Å |
| b | 14.557 ± 0.003 Å |
| c | 17.393 ± 0.003 Å |
| α | 94.102 ± 0.004° |
| β | 105.644 ± 0.004° |
| γ | 101.451 ± 0.003° |
| Cell volume | 2947.4 ± 0.9 Å3 |
| Cell temperature | 293 K |
| Ambient diffraction temperature | 293 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1184 |
| Residual factor for significantly intense reflections | 0.0705 |
| Weighted residual factors for significantly intense reflections | 0.1829 |
| Weighted residual factors for all reflections included in the refinement | 0.2172 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.015 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 190774 (current) | 2017-01-20 | cif/ Adding structures of 7227482, 7227483, 7227484, 7227485 via cif-deposit CGI script. |
7227482.cif |
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