Crystallography Open Database

Information card for entry 7229799

Preview

Coordinates	7229799.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H49 Dy2 F12 N2 O12
Calculated formula	C64 H49 Dy2 F12 N2 O12
Title of publication	A series of salen-type asymmetric dinuclear Dy(iii) complexes: site-resolved two-step magnetic relaxation process
Authors of publication	Zhang, Wan-Ying; Chen, Peng; Tian, Yong-Mei; Li, Hong-Feng; Sun, Wen-Bin; Yan, Peng-Fei
Journal of publication	CrystEngComm
Year of publication	2018
Journal volume	20
Journal issue	6
Pages of publication	777
a	10.7743 ± 0.0003 Å
b	13.7731 ± 0.0004 Å
c	21.4829 ± 0.0006 Å
α	94.837 ± 0.002°
β	90.373 ± 0.002°
γ	95.881 ± 0.002°
Cell volume	3159.52 ± 0.16 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.105
Residual factor for significantly intense reflections	0.0679
Weighted residual factors for significantly intense reflections	0.1304
Weighted residual factors for all reflections included in the refinement	0.1459
Goodness-of-fit parameter for all reflections included in the refinement	1.127
Diffraction radiation wavelength	0.71 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229009 (current)	2019-11-17	cif/ Updating files of 7229799, 7229800, 7229801, 7229802 Original log message: Adding full bibliography for 7229799--7229802.cif.	7229799.cif
204536	2017-12-27	cif/ Adding structures of 7229799, 7229800, 7229801, 7229802 via cif-deposit CGI script.	7229799.cif