Crystallography Open Database

Information card for entry 7230209

Preview

Coordinates	7230209.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C7 H22 O3 Si3
Calculated formula	C7 H22 O3 Si3
Title of publication	Aerobic Co or Cu/NHPI-catalyzed oxidation of hydride siloxanes: synthesis of siloxanols
Authors of publication	Arzumanyan, Ashot V.; Goncharova, Irina K.; Novikov, Roman A.; Milenin, Sergey A.; Boldyrev, Konstantin L.; Solyev, Pavel N.; Tkachev, Yaroslav V.; Volodin, Alexander D.; Smol'yakov, Alexander F.; Korlyukov, Alexander A.; Muzafarov, Aziz M.
Journal of publication	Green Chemistry
Year of publication	2018
Journal volume	20
Journal issue	7
Pages of publication	1467
a	17.5199 ± 0.0018 Å
b	17.5199 ± 0.0018 Å
c	10.0567 ± 0.0014 Å
α	90°
β	90°
γ	90°
Cell volume	3086.9 ± 0.6 Å³
Cell temperature	230 K
Ambient diffraction temperature	230 K
Number of distinct elements	4
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.1323
Residual factor for significantly intense reflections	0.05
Weighted residual factors for significantly intense reflections	0.1118
Weighted residual factors for all reflections included in the refinement	0.1359
Goodness-of-fit parameter for all reflections included in the refinement	0.945
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
230108 (current)	2019-11-17	cif/ Updating files of 7230209 Original log message: Adding full bibliography for 7230209.cif.	7230209.cif
206710	2018-03-01	cif/ Adding structures of 7230209 via cif-deposit CGI script.	7230209.cif